詳細(xì)介紹
島津Shim-pack GIS C18制備色譜柱
高效液相色譜( HPLC)是實驗室常用的分離分析手段,用于復(fù)雜樣品中目標(biāo)組分的定性和定量分析。按照樣品分離的目的和規(guī)模區(qū)分,高效液相色譜可以分為分析型和制備型。與分析性HPLC不同的是,制備型HPLC不僅要獲得樣品分離的譜圖,更重要的是對樣品中的目標(biāo)組分或目標(biāo)化合物進(jìn)行收集,獲得達(dá)到一定純度要求的餾分,以備后續(xù)研究和生產(chǎn)使用,所以其檢測器末端通常會連接餾分收集器對目標(biāo)組分予以收集。
制備型高效液相色譜主要應(yīng)用在植物化學(xué)、藥物合成、生物化學(xué)等領(lǐng)域的產(chǎn)品的提取及純化工作中。不同的工作領(lǐng)域中組分的制備和純化量的差異較大。在生物技術(shù)領(lǐng)域中,酶的分離是μg級;在天然產(chǎn)物化學(xué)和合成化學(xué)領(lǐng)域中,為應(yīng)對未知成分定性鑒別、結(jié)構(gòu)測定、生物活性測試等要求,需要純化若干mg級的高純物;在藥品和醫(yī)藥學(xué)測試中,需要g級的標(biāo)準(zhǔn)品和對照品;在工業(yè)級提純中,目標(biāo)產(chǎn)物工業(yè)化生產(chǎn)往往需要kg級的分離純化。
我們島津技邇公司擁有強(qiáng)da色譜柱研發(fā)實力,從微量分析的毛細(xì)管液相柱,到常規(guī)分析柱,再到不同量級的制備放大,我們都能為您一站式提供!而且色譜柱的填料種類選擇豐富,涵蓋多種分離模式,能夠滿足多種分析需求!
Shim-pack GIS C18系列由于其顯著的低壓力、高保留、通用性強(qiáng)的特性而深受廣大客戶的歡迎,GIS系列5μm, 10um 制備柱更是由于其高效,高分離度,高性價比而成為我們的guan軍銷量制備柱!
性能參數(shù):
鍵合相: | 十八烷基 | 粒徑選擇: | 5um,10um |
孔徑: | 100? | 比表面積: | 450m2/g |
含碳量: | 15% | 端基封尾: | * |
pH范圍: | 2-7.5 | USP固定相: | L1 |
產(chǎn)品特點:
1. 高樣品負(fù)載:填料具有450m2/g的大表面積,能夠大幅增加每次制備的樣品量,可降低樣品注入次數(shù),減少溶劑量的使用成本!
2. 高惰性:實施高度端基封尾,可很好的抑制酸性、堿性化合物吸附,減少拖尾現(xiàn)象!
3. 低柱壓:填料粒徑分布均勻,即使采用甲醇流動相,也能保持低壓力!
4. 簡易的規(guī)模放大:制備尺寸,具有與分析色譜柱同等的性能,可以在分析方法開發(fā)的條件下快速簡便是的實現(xiàn)無縫放大!
應(yīng)用例:
Shim-pack GIS C18制備柱
分析條件:
色譜柱:Shim-pack GIS C18
流動相:A:CH3CN B:H2O A/B=65:35 v/v
柱溫:40 ℃
檢測:UV 254nm
樣品: 1.苯乙酮 2.苯 3.甲苯 4.萘
訂貨信息:
制備柱:
227-30107-01 | Shim-pack GIS C18, 5um, 6.0x50 |
227-30107-02 | Shim-pack GIS C18, 5um, 6.0x150 |
227-30107-03 | Shim-pack GIS C18, 5um, 6.0x250 |
227-30107-04 | Shim-pack GIS C18, 5um, 6.0x100 |
227-30107-05 | Shim-pack GIS C18, 5um, 7.6x50 |
227-30107-06 | Shim-pack GIS C18, 5um, 7.6x100 |
227-30107-07 | Shim-pack GIS C18, 5um, 7.6x150 |
227-30107-08 | Shim-pack GIS C18, 5um, 7.6x250 |
227-30108-01 | Shim-pack GIS C18, 5um, 10x50 |
227-30108-02 | Shim-pack GIS C18, 5um, 10x100 |
227-30108-03 | Shim-pack GIS C18, 5um, 10x150 |
227-30108-04 | Shim-pack GIS C18, 5um, 10x250 |
227-30108-05 | Shim-pack GIS C18, 5um, 14x50 |
227-30108-06 | Shim-pack GIS C18, 5um, 14x150 |
227-30108-07 | Shim-pack GIS C18, 5um, 14x250 |
227-30109-01 | Shim-pack GIS C18, 5um, 20x50 |
227-30109-02 | Shim-pack GIS C18, 5um, 20x100 |
227-30109-03 | Shim-pack GIS C18, 5um, 20x150 |
227-30109-04 | Shim-pack GIS C18, 5um, 20x250 |
227-30110-01 | Shim-pack GIS C18, 5um, 30x50 |
227-30110-02 | Shim-pack GIS C18, 5um, 30x100 |
227-30110-03 | Shim-pack GIS C18, 5um, 30x150 |
227-30110-04 | Shim-pack GIS C18, 5um, 30x250 |
227-30110-05 | Shim-pack GIS C18, 5um, 50x250 |
227-30111-01 | Shim-pack GIS C18, 10um, 4.0x150 |
227-30111-02 | Shim-pack GIS C18, 10um, 4.0x250 |
227-30112-01 | Shim-pack GIS C18, 10um, 4.6x150 |
227-30112-02 | Shim-pack GIS C18, 10um, 4.6x250 |
227-30113-01 | Shim-pack GIS C18, 10um, 10x50 |
227-30113-02 | Shim-pack GIS C18, 10um, 10x100 |
227-30113-03 | Shim-pack GIS C18, 10um, 10x150 |
227-30113-04 | Shim-pack GIS C18, 10um, 10x250 |
227-30114-01 | Shim-pack GIS C18, 10um, 14x50 |
227-30114-02 | Shim-pack GIS C18, 10um, 14x100 |
227-30114-03 | Shim-pack GIS C18, 10um, 14x150 |
227-30114-04 | Shim-pack GIS C18, 10um, 14x250 |
227-30115-01 | Shim-pack GIS C18, 10um, 20x50 |
227-30115-02 | Shim-pack GIS C18, 10um, 20x100 |
227-30115-03 | Shim-pack GIS C18, 10um, 20x150 |
227-30115-04 | Shim-pack GIS C18, 10um, 20x250 |
227-30116-01 | Shim-pack GIS C18, 10um, 30x50 |
227-30116-02 | Shim-pack GIS C18, 10um, 30x100 |
227-30116-03 | Shim-pack GIS C18, 10um, 30x150 |
227-30116-04 | Shim-pack GIS C18, 10um, 30x250 |
227-30116-05 | Shim-pack GIS C18, 10um, 50x250 |
保護(hù)柱:
227-30137-01 | Shim-pack GIS (G) C18, 5um, 6.0x50 |
227-30138-01 | Shim-pack GIS (G) C18, 5um, 7.6x50 |
227-30139-01 | Shim-pack GIS (G) C18, 5um, 10x50 |
227-30140-01 | Shim-pack GIS (G) C18, 5um, 14x50 |
227-30141-01 | Shim-pack GIS (G) C18, 5um, 20x50 |
227-30142-01 | Shim-pack GIS (G) C18, 5um, 30x50 |
227-30143-01 | Shim-pack GIS (G) C18, 5um, 50x75 |
227-30144-01 | Shim-pack GIS (G) C18, 10um, 10x50 |
227-30145-01 | Shim-pack GIS (G) C18, 10um, 14x50 |
227-30146-01 | Shim-pack GIS (G) C18, 10um, 20x50 |
227-30147-01 | Shim-pack GIS (G) C18, 10um, 30x50 |
227-30148-01 | Shim-pack GIS (G) C18, 10um, 50x75 |
島津Shim-pack GIS C18制備色譜柱
高效液相色譜( HPLC)是實驗室常用的分離分析手段,用于復(fù)雜樣品中目標(biāo)組分的定性和定量分析。按照樣品分離的目的和規(guī)模區(qū)分,高效液相色譜可以分為分析型和制備型。與分析性HPLC不同的是,制備型HPLC不僅要獲得樣品分離的譜圖,更重要的是對樣品中的目標(biāo)組分或目標(biāo)化合物進(jìn)行收集,獲得達(dá)到一定純度要求的餾分,以備后續(xù)研究和生產(chǎn)使用,所以其檢測器末端通常會連接餾分收集器對目標(biāo)組分予以收集。
制備型高效液相色譜主要應(yīng)用在植物化學(xué)、藥物合成、生物化學(xué)等領(lǐng)域的產(chǎn)品的提取及純化工作中。不同的工作領(lǐng)域中組分的制備和純化量的差異較大。在生物技術(shù)領(lǐng)域中,酶的分離是μg級;在天然產(chǎn)物化學(xué)和合成化學(xué)領(lǐng)域中,為應(yīng)對未知成分定性鑒別、結(jié)構(gòu)測定、生物活性測試等要求,需要純化若干mg級的高純物;在藥品和醫(yī)藥學(xué)測試中,需要g級的標(biāo)準(zhǔn)品和對照品;在工業(yè)級提純中,目標(biāo)產(chǎn)物工業(yè)化生產(chǎn)往往需要kg級的分離純化。
我們島津技邇公司擁有強(qiáng)da色譜柱研發(fā)實力,從微量分析的毛細(xì)管液相柱,到常規(guī)分析柱,再到不同量級的制備放大,我們都能為您一站式提供!而且色譜柱的填料種類選擇豐富,涵蓋多種分離模式,能夠滿足多種分析需求!
Shim-pack GIS C18系列由于其顯著的低壓力、高保留、通用性強(qiáng)的特性而深受廣大客戶的歡迎,GIS系列5μm, 10um 制備柱更是由于其高效,高分離度,高性價比而成為我們的guan軍銷量制備柱!
性能參數(shù):
鍵合相: | 十八烷基 | 粒徑選擇: | 5um,10um |
孔徑: | 100? | 比表面積: | 450m2/g |
含碳量: | 15% | 端基封尾: | * |
pH范圍: | 2-7.5 | USP固定相: | L1 |
產(chǎn)品特點:
1. 高樣品負(fù)載:填料具有450m2/g的大表面積,能夠大幅增加每次制備的樣品量,可降低樣品注入次數(shù),減少溶劑量的使用成本!
2. 高惰性:實施高度端基封尾,可很好的抑制酸性、堿性化合物吸附,減少拖尾現(xiàn)象!
3. 低柱壓:填料粒徑分布均勻,即使采用甲醇流動相,也能保持低壓力!
4. 簡易的規(guī)模放大:制備尺寸,具有與分析色譜柱同等的性能,可以在分析方法開發(fā)的條件下快速簡便是的實現(xiàn)無縫放大!
應(yīng)用例:
Shim-pack GIS C18制備柱
分析條件:
色譜柱:Shim-pack GIS C18
流動相:A:CH3CN B:H2O A/B=65:35 v/v
柱溫:40 ℃
檢測:UV 254nm
樣品: 1.苯乙酮 2.苯 3.甲苯 4.萘
訂貨信息:
制備柱:
227-30107-01 | Shim-pack GIS C18, 5um, 6.0x50 |
227-30107-02 | Shim-pack GIS C18, 5um, 6.0x150 |
227-30107-03 | Shim-pack GIS C18, 5um, 6.0x250 |
227-30107-04 | Shim-pack GIS C18, 5um, 6.0x100 |
227-30107-05 | Shim-pack GIS C18, 5um, 7.6x50 |
227-30107-06 | Shim-pack GIS C18, 5um, 7.6x100 |
227-30107-07 | Shim-pack GIS C18, 5um, 7.6x150 |
227-30107-08 | Shim-pack GIS C18, 5um, 7.6x250 |
227-30108-01 | Shim-pack GIS C18, 5um, 10x50 |
227-30108-02 | Shim-pack GIS C18, 5um, 10x100 |
227-30108-03 | Shim-pack GIS C18, 5um, 10x150 |
227-30108-04 | Shim-pack GIS C18, 5um, 10x250 |
227-30108-05 | Shim-pack GIS C18, 5um, 14x50 |
227-30108-06 | Shim-pack GIS C18, 5um, 14x150 |
227-30108-07 | Shim-pack GIS C18, 5um, 14x250 |
227-30109-01 | Shim-pack GIS C18, 5um, 20x50 |
227-30109-02 | Shim-pack GIS C18, 5um, 20x100 |
227-30109-03 | Shim-pack GIS C18, 5um, 20x150 |
227-30109-04 | Shim-pack GIS C18, 5um, 20x250 |
227-30110-01 | Shim-pack GIS C18, 5um, 30x50 |
227-30110-02 | Shim-pack GIS C18, 5um, 30x100 |
227-30110-03 | Shim-pack GIS C18, 5um, 30x150 |
227-30110-04 | Shim-pack GIS C18, 5um, 30x250 |
227-30110-05 | Shim-pack GIS C18, 5um, 50x250 |
227-30111-01 | Shim-pack GIS C18, 10um, 4.0x150 |
227-30111-02 | Shim-pack GIS C18, 10um, 4.0x250 |
227-30112-01 | Shim-pack GIS C18, 10um, 4.6x150 |
227-30112-02 | Shim-pack GIS C18, 10um, 4.6x250 |
227-30113-01 | Shim-pack GIS C18, 10um, 10x50 |
227-30113-02 | Shim-pack GIS C18, 10um, 10x100 |
227-30113-03 | Shim-pack GIS C18, 10um, 10x150 |
227-30113-04 | Shim-pack GIS C18, 10um, 10x250 |
227-30114-01 | Shim-pack GIS C18, 10um, 14x50 |
227-30114-02 | Shim-pack GIS C18, 10um, 14x100 |
227-30114-03 | Shim-pack GIS C18, 10um, 14x150 |
227-30114-04 | Shim-pack GIS C18, 10um, 14x250 |
227-30115-01 | Shim-pack GIS C18, 10um, 20x50 |
227-30115-02 | Shim-pack GIS C18, 10um, 20x100 |
227-30115-03 | Shim-pack GIS C18, 10um, 20x150 |
227-30115-04 | Shim-pack GIS C18, 10um, 20x250 |
227-30116-01 | Shim-pack GIS C18, 10um, 30x50 |
227-30116-02 | Shim-pack GIS C18, 10um, 30x100 |
227-30116-03 | Shim-pack GIS C18, 10um, 30x150 |
227-30116-04 | Shim-pack GIS C18, 10um, 30x250 |
227-30116-05 | Shim-pack GIS C18, 10um, 50x250 |
保護(hù)柱:
227-30137-01 | Shim-pack GIS (G) C18, 5um, 6.0x50 |
227-30138-01 | Shim-pack GIS (G) C18, 5um, 7.6x50 |
227-30139-01 | Shim-pack GIS (G) C18, 5um, 10x50 |
227-30140-01 | Shim-pack GIS (G) C18, 5um, 14x50 |
227-30141-01 | Shim-pack GIS (G) C18, 5um, 20x50 |
227-30142-01 | Shim-pack GIS (G) C18, 5um, 30x50 |
227-30143-01 | Shim-pack GIS (G) C18, 5um, 50x75 |
227-30144-01 | Shim-pack GIS (G) C18, 10um, 10x50 |
227-30145-01 | Shim-pack GIS (G) C18, 10um, 14x50 |
227-30146-01 | Shim-pack GIS (G) C18, 10um, 20x50 |
227-30147-01 | Shim-pack GIS (G) C18, 10um, 30x50 |
227-30148-01 | Shim-pack GIS (G) C18, 10um, 50x75 |